HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl-phenyl-carbamic Acid 4-(2-hydroxy-ethyl)-phenyl Ester → Methyl-phenyl-carbamic Acid 4-(2-tetrazol-1-yl-ethyl)-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl-phenyl-carbamic Acid 4-(2-hydroxy-ethyl)-phenyl Ester | HCID 69520342 | — |
| Reactant | HCID 178418441 | HCID 178418441 | — |
| Product | Methyl-phenyl-carbamic Acid 4-(2-tetrazol-1-yl-ethyl)-phenyl Ester | HCID 69519158 | 10% |
Reaction Steps
The title compound was prepared in 10% yield as an oil using methyl-phenyl-carbamic acid 4-(2-hydroxy-ethyl)-phenyl ester and tetrazole. NMR (400 MHz; CDCl3): δ 3.19 (t, 2H), 3.40 (br s, 3H), 3.47 (s, 1H), 4.61 (t, 2H), 6.98-7.07 (m, 4H), 7.25-7.42 (m, 5H), 8.26 (s, 1H); HPLC-MS: m/z=324.1 (M+1); Rt=3.36 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-cb8ba2f209bb45bcabd91f7fea9de85c |
| Source note | uspto-grants-2007_10 |