HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 86618214, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 86618215 | HCID 86618215 | — |
| Product | HCID 86618214 | HCID 86618214 | — |
Reaction Steps
The title compound was prepared by reacting 4′-{[tert-butyl(dimethyl)silyl]oxy}-3-chloro-1,1′-biphenyl-4-carbaldehyde (405 mg, 1.17 mmol) with hydroxylamine hydrochloride (154 mg, 2.22 mmol) according to Method C to yield a yellowish oil which was used in the next step without purification: MS (ESI) m/z 362/364 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279600B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-fbdc00e75e824360a105e18abb94ab94 |
| Source note | uspto-grants-2007_10 |