Hydroxyamine hydrochloride → HCID 86596213, compound

Participants

Reaction Steps

The title compound was prepared by reacting 4′-{[tert-butyl(dimethyl)silyl]oxy}-2-fluoro-1,1′-biphenyl-4-carbaldehyde (450 mg, 1.36 mmol) with hydroxylamine hydrochloride (190 mg, 2.73 mmol) according to Method C to yield a white solid which was used in the next step without purification: MS (ESI) m/z 344 (M−H)−, 346 (M+H)+.

Provenance & Evidence