4-Bromo-2-fluorobenzaldehyde → HCID 23005036, compound

Participants

Reaction Steps

The title compound was prepared by reacting 4-bromo-2-fluoro-benzaldehyde (3 g, 14.8 mmol) with 4-methoxyphenylboronic acid (2.70 g, 17.8 mmol) according to Method B to yield 3.2 g (94%) of white solid: mp 85-86° C.; 1H NMR (DMSO-d6): δ 3.83 (3H, s). 7.06-7.09 (2H, m), 7.70-7.75 (2H, m), 7.79-7.82 (2H, m), 7.88 (1H, t, J=7.96 Hz), 10.22 (1H, s); IR 1681 cm−1; MS (ESI) m/z 231 (M+H)+.

Provenance & Evidence