Hydroxyamine hydrochloride → HCID 136338596, compound

Participants

Reaction Steps

The title compound was prepared by reacting 4′-hydroxy[1,1′-biphenyl]-4-carbaldehyde (1.03 mmol) with hydroxylamine hydrochloride (140 mg, 2 mmol) according to Method C to yield 193 mg (79%, over two steps) of yellowish solid: mp 207-210° C.; 1H NMR (DMSO-d6): δ 6.85 (2H, d, J=8.37 Hz), 7.53 (2H, d, J=8.39 Hz), 7.62 (4H, s), 8.15 (1H, s), 9.62 (1H, s), 11.21 (1H, s); MS (ESI) m/z 212 (M−H)−.

Provenance & Evidence