HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromopyridine → (4-Bromophenyl)(pyridin-2-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromopyridine | HCID 7973 | — |
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Product | (4-Bromophenyl)(pyridin-2-yl)methanol | HCID 12177878 | — |
Reaction Steps
Using the same protocol as described in example 22, step 1, 2-bromopyridine (477 μL, 5.0 mmol) was added to 4-bromobenzaldehyde (1.018 g, 5.5 mmol). The crude residue obtained was chromatographed on silica gel using 50% ethyl acetate in hexanes to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279478B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-50a55c57eb3f493799c4498219d8cbd3 |
| Source note | uspto-grants-2007_10 |