HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromopyridine → (4-Bromophenyl)(pyridin-3-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromopyridine | HCID 12286 | — |
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Product | (4-Bromophenyl)(pyridin-3-yl)methanol | HCID 13282976 | — |
Reaction Steps
Using the same protocol as described in example 22, step 1, 3-bromopyridine (482 μL, 5.0 mmol) was added to 4-bromobenzaldehyde (1.018 g, 5.5 mmol). The crude residue was chromatographed on silica gel using 1% NH4OH and 9% MeOH in dichloromethane to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279478B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-b7547f18c75e4ae98d84d5b629f8a184 |
| Source note | uspto-grants-2007_10 |