HuagongsheHuagongshe Chemistry Print Report · For research reference only
PyridiuM iodide → HCID 86605390, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | PyridiuM iodide | HCID 21863515 | — |
| Reactant | HCID 86605392 | HCID 86605392 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86605390 | HCID 86605390 | — |
Reaction Steps
Using the same procedure as described for example 36 step 3 (2S)-N-(cyanomethyl)-4-methyl-2-{[(R)-phenyl(4-pyridin-3-ylphenyl)methyl]oxy}pentanamide (150 mg, 0.36 mmol) was converted to its pyridinium iodide salt. The salt was swished with diethyl ether (20 mL) for 18 h and the title compound was filtered off as an amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279478B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-e30aefd40606435fa8c362933bc42027 |
| Source note | uspto-grants-2007_10 |