HCID 178480808, compound → HCID 178480809, compound

HRID 1180465Notes

Reaction equation

HRID 1180465 reaction equation
[Cl-:1].[CH3:2][N:3]1[CH:7]=[CH:6][N+:5]([CH3:8])=[C:4]1/[N:9]=[N:10]/[C:11]1[CH:16]=[CH:15][C:14]([N:17]2[CH2:22][CH2:21][NH:20][CH2:19][CH2:18]2)=[CH:13][CH:12]=1>CN(C=O)C.BrCCCCCCBr>[Cl-:1].[CH3:8][N:5]1[CH:6]=[CH:7][N+:3]([CH3:2])=[C:4]1/[N:9]=[N:10]/[C:11]1[CH:12]=[CH:13][C:14]([N:17]2[CH2:18][CH2:19][N:20]([CH2:15][CH2:16][CH2:11][CH2:12][CH2:13][CH2:14][N:20]3[CH2:21][CH2:22][N:17]([C:14]4[CH:13]=[CH:12][C:11](/[N:10]=[N:9]/[C:4]5[N:5]([CH3:8])[CH:6]=[CH:7][N+:3]=5[CH3:2])=[CH:16][CH:15]=4)[CH2:18][CH2:19]3)[CH2:21][CH2:22]2)=[CH:15][CH:16]=1.[Cl-:1]

Participants

4

Reactant 1

HCID 178480808HCID 178480808, compound

Product 1

HCID 178480809HCID 178480809, compound

Reagents, catalysts & solvents 2

HCID 6228DimethylformamideSolventHCID 123681,6-DibromohexaneSolvent

Procedure

2-[(E)(4-{4-[6-(4-{4-[(E)(1,3-dimethyl-1H-imidazol-3-ium-2-yl)diazenyl]phenyl}piperazin-1-yl)hexyl]piperazin-1-yl}phenyl)diazenyl]-1,3-dimethyl-1H-imidazol-3-ium chloride (I) was synthesized by dissolving 1,3-Dimethyl-2-[(E)(4-piperazin-1-ylphenyl)diazenyl]-1H-imidazol-3-ium chloride (0.9 g) in DMF (20 ml), Br(CH2)6Br (0.5 mol

Sources & evidence

ORD record
ord-1e6c142d8de9420e92b955cfaed61e47
Source dataset
uspto-grants-2007_10
Patent number
US07282068B2

Reaction notes

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