HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1180467Generated: November 1, 2026
Carbamic acid, ethyl ester → Toluene 2,4-Diisocyanate
https://huagongshe.com/reaction/1180467
Participants
| Role | Name | HCID | Charge |
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| Reactant | Carbamic acid, ethyl ester | HCID 5641 | — |
| Reactant | Isocyanate | HCID 105034 | — |
| Reactant | HCID 21226399 | HCID 21226399 | — |
| Product | Toluene 2,4-Diisocyanate | HCID 11443 | — |
| Product | Hexamethylene diisocyanate | HCID 13192 | — |
Reaction Steps
As the adhesive layer, a polyester-urethane adhesive was used and a composition for an adhesive layer was prepared as follows. That is, a polyester resin (80 parts by weight, VYLON RV-200) manufactured by Toyo Boseki Kabushiki Kaisha was dissolved in a mixed solvent (1940 parts by weight) of toluene/methyl ethyl ketone=80/20 (weight ratio) while heating at 80° C. After cooling, DESMODUER HL (20 parts by weight, manufactured by Sumitomo Bayer Urethane) which is isocyanulate polyhydric isocyanate obtained from hexamethylene diisocyanate and toluene diisocyanate as starting materials, was added as isocyanulate polyhydric isocyanate, and triethylene diamine (0.06 part by weight) was added as a curing catalyst, and the mixture was stirred for 10 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07282256B2 |
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| Source dataset | uspto-grants-2007_10 |
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| ORD ID | ord-8659fbfd7f1f433a9d32e19c4317adcd |
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| Source note | uspto-grants-2007_10 |
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