5-Chloro-3-phenyl-1,2,4-thiadiazole → (1-{[(3-Phenyl-1,2,4-thiadiazol-5-yl)oxy]methyl}cyclobutyl)methanol

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Reaction Steps

The title compound was prepared using the same experimental procedure as in example 25a from [1-(hydroxymethyl)cyclobutyl]methanol and 5-chloro-3-phenyl-1,2,4-thiadiazole. 1H NMR (300 MHz, CDCl3) δ 8.10 (m, 2H), 7.39 (m, 3H), 4.63 (s, 2H), 3.62 (d, J=6 Hz, 2H), 2.71 (t, J=6 Hz, 1H), 1.88-1.97 (m, 6H). GC-MS m/z 277 (M+H).

Provenance & Evidence