Cyclobutane-1,1-diyldimethanol → HCID 11266095, compound

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Reaction Steps

The title compound was prepared using the same experimental procedure as in example 25a from [1-(hydroxymethyl)cyclobutyl]methanol and 3-chloro-6-methyl-4-phenylpyridazine. 1H NMR (300 MHz, CDCl3) δ 7.58-7.25 (m, 6H), 4.64 (s, 2H), 3.59 (d, J=6 Hz, 2H), 3.05 (t, J=7 Hz, 1H), 2.63 (s, 3H), 2.00-1.73 (m, 6H). GC-MS m/z 285 (M+H).

Provenance & Evidence