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m-Chloroperbenzoic acid → HCID 178526236、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | m-Chloroperbenzoic acid | HCID 70297 | — |
| 反応物 | 4-Bromo-1H-pyrrolo[2,3-b]pyridine | HCID 22273643 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | HCID 178526236 | HCID 178526236 | 87% |
反応手順
To a solution of 4-bromo-1H-pyrrolo[2,3-b]pyridine (25 mmol) in diethyl ether (400 mL) under nitrogen at room temperature was added m-chloroperbenzoic acid (40 mmol). The reaction was stirred for 2.5 h. The resultant precipitate was filtered and washed with cold ether (50 mL) to give the title compound as an off-white solid (87%). ESMS[M+H]+: 213.2
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07282588B2 |
| 出典データセット | uspto-grants-2007_10 |
| ORD ID | ord-83238d034b8c4e38958dcd8fa1046abd |
| 出典メモ | uspto-grants-2007_10 |