HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 68995203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | 2-(Ethylamino)ethanol | HCID 8072 | — |
| Reactant | HCID 86613331 | HCID 86613331 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 68995203 | HCID 68995203 | — |
Reaction Steps
Following the procedure described in Intermediate 101 using N-(4-{4-[2-(4-formylphenyl)-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-1-methyl-1H-pyrazol-3-yl}phenyl)-1-pyrrolidinecarboxamide and 2-(ethylamino)ethanol in dichloroethane (instead of dichloromethane) provided the title compound. ESMS [M+H]+: 704.6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07282588B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-4582b61f71784da1bdae75c7dbb352e5 |
| Source note | uspto-grants-2007_10 |