HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58979123, compound → HCID 58979222, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58979123 | HCID 58979123 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58979222 | HCID 58979222 | — |
Reaction Steps
A solution of 3-[4-benzyloxy-3-(tert-butoxycarbonylamino-methyl)-phenyl]-propionic acid methyl ester (8.50 g, 21.3 mmol) in THF (100 mL) was treated with 5% Pd-on-carbon (1.1 g) and shaken under a hydrogen atmosphere (60 psi) at ambient temperature for 6 h. The mixture was filtered through Celite and concentrated to a pale yellow solid (5.63 g, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07282501B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-3e57fbb893fd46e89caf5a88c6af2873 |
| Source note | uspto-grants-2007_10 |