HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 54211444, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Diethylphosphite | HCID 3780918 | — |
| Reactant | HCID 136186576 | HCID 136186576 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 54211444 | HCID 54211444 | — |
Reaction Steps
Triethylamine (1.1 mmol) was added slowly to an ice-cooled solution of. 6-chloro-N9-neopentyl-8-(2-hydroxyphenyl)purine (1 mmol) and diethyl phosphite (1 mmol) in carbontetrachloride. The reaction was stirred at room temperature overnight. Triethylamine hydrochloride was precipitated as a white solid mass. Extraction and chromatography gave diethyl 2-(6-Chloro-N9-neopentylpurin-8-yl)phenyl phosphate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07285543B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-7dfcd6fa2bbc48269d168d5ee4ddecec |
| Source note | uspto-grants-2007_10 |