HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromo-2-methylpropane → 5-methyl-2-(1-naphthylmethyl)-7-neopentyl-3-pyridin-4-yl-2H-pyrazolo[3,4-d]pyrimidine-4,6(5H,7H)-dione
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromo-2-methylpropane | HCID 6555 | — |
| Edukt | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Edukt | 5-methyl-2-(1-naphthylmethyl)-3-(4-pyridinyl)-2H-pyrazolo[3,4-d]pyrimidine-4,6(5H,7H)-dione | HCID 136334113 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | 5-methyl-2-(1-naphthylmethyl)-7-neopentyl-3-pyridin-4-yl-2H-pyrazolo[3,4-d]pyrimidine-4,6(5H,7H)-dione | HCID 58981076 | — |
Reaktionsschritte
This compound was synthesized by the reaction of 5-methyl-2-(1-naphthylmethyl)-3-pyridin-4-yl-2H-pyrazolo[3,4-d]pyrimidine-4,6(5H,7H)-dione and 1-bromo-2-methylpropane using DBU as abase in DMF at 100° C. Mass: 454.36 (M+H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07285558B2 |
| Quelldatensatz | uspto-grants-2007_10 |
| ORD ID | ord-943e9caeb6a9418989d3fc01f4dc0a6e |
| Quellennotiz | uspto-grants-2007_10 |