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HRID1181747

反应详情

EQUATION

反应方程式

HRID 1181747 的结构方程式

REACTANTS

反应物

3
结构：CC(C)CBr
HCID6555

1-Bromo-2-methylpropane

C4H9Br

结构：C1CCC2=NCCCN2CC1
HCID81184

1,8-Diazabicyclo[5.4.0]undec-7-ene

C9H16N2

结构：Cn1c(=O)[nH]c2nn(Cc3cccc4ccccc34)c(-c3ccncc3)c2c1=O
HCID136334113

未命名化合物

PRODUCTS

生成物

1
结构：Cn1c(=O)c2c(-c3ccncc3)n(Cc3cccc4ccccc34)nc2n(CC(C)(C)C)c1=O
HCID58981076

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

This compound was synthesized by the reaction of 5-methyl-2-(1-naphthylmethyl)-3-pyridin-4-yl-2H-pyrazolo[3,4-d]pyrimidine-4,6(5H,7H)-dione and 1-bromo-2-methylpropane using DBU as abase in DMF at 100° C. Mass: 454.36 (M+H).

WORKUP

后处理

  1. customat 100° C