HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → 7-(4-hydroxybenzyl)-5-methyl-2-(1-naphthylmethyl)-3-pyridin-4-yl-2H-pyrazolo[3,4-d]pyrimidine-4,6(5H,7H)-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | 4-{[5-methyl-2-(1-naphthylmethyl)-4,6-dioxo-3-pyridin-4-yl-2,4,5,6-tetrahydro-7H-pyrazolo[3,4-d]pyrimidin-7-yl]methyl}phenyl acetate | HCID 69428081 | — |
| Product | 7-(4-hydroxybenzyl)-5-methyl-2-(1-naphthylmethyl)-3-pyridin-4-yl-2H-pyrazolo[3,4-d]pyrimidine-4,6(5H,7H)-dione | HCID 58980990 | — |
Reaction Steps
This compound was synthesized by the hydrolysis of 4-{[5-methyl-2-(1-naphthylmethyl)-4,6-dioxo-3-pyridin-4-yl-2,4,5,6-tetrahydro-7H-pyrazolo[3,4-d]pyrimidin-7-yl]methyl}phenyl acetate with 0.5N LiOH at room temperature for six hours. Mass: 489.80 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07285558B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-84292c1239ec42d7a11a5584b753e944 |
| Source note | uspto-grants-2007_10 |