Lithium Hydroxide → HCID 58981057, compound

HRID 1181776Notes

Reaction equation

[CH3:1][N:2]1[C:7](=[O:8])[C:6]2=[C:9]([C:23]3[CH:28]=[CH:27][N:26]=[CH:25][CH:24]=3)[N:10]([CH2:12][C:13]3[C:22]4[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=4)[CH:16]=[CH:15][CH:14]=3)[N:11]=[C:5]2[N:4]([CH2:29][C:30]2[CH:31]=[C:32]([CH:37]=[CH:38][CH:39]=2)[C:33]([O:35]C)=[O:34])[C:3]1=[O:40].[Li+].[OH-]>>[CH3:1][N:2]1[C:7](=[O:8])[C:6]2=[C:9]([C:23]3[CH:24]=[CH:25][N:26]=[CH:27][CH:28]=3)[N:10]([CH2:12][C:13]3[C:22]4[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=4)[CH:16]=[CH:15][CH:14]=3)[N:11]=[C:5]2[N:4]([CH2:29][C:30]2[CH:31]=[C:32]([CH:37]=[CH:38][CH:39]=2)[C:33]([OH:35])=[O:34])[C:3]1=[O:40]

Participants

Reactant 2

HCID 3939Lithium Hydroxide

HCID 69429562HCID 69429562, compound

Product 1

HCID 58981057HCID 58981057, compound

Procedure

This compound was synthesized by the hydrolysis of methyl 3-{[5-methyl-2-(1-naphthylmethyl)-4,6-dioxo-3-pyridin-4-yl-2,4,5,6-tetrahydro-7H-pyrazolo[3,4-d]pyrimidin-7-yl]methyl}benzoate with 0.5N LiOH at room temperature for eight hours. Mass: 517.79 (M+H).

Sources & evidence

ORD record: ord-329a152805284b90aebdf40fa24dd43c
Source dataset: uspto-grants-2007_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07285558B2

Reaction notes

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