HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 59643717, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 59643727 | HCID 59643727 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59643717 | HCID 59643717 | — |
Reaction Steps
To a solution of 47 (75 mg) in dichloromethane (5 mL) was added TFA (0.5 mL). The solution was stirred overnight. Followed by usual workup. The title compound was obtained as an off-white solid (35 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07288538B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-d2d24c2b46c04486a30897f8c997ac00 |
| Source note | uspto-grants-2007_10 |