HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfide → HCID 178439422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfide | HCID 1068 | — |
| Reactant | Boron trifluoride | HCID 6356 | — |
| Reactant | HCID 178492477 | HCID 178492477 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178439422 | HCID 178439422 | — |
Reaction Steps
A reaction mixture of 3,5-dichloro-4-(4-methoxy-3-isopropylphenoxy)-benzyltetrazole (60 mg), BF3.Me2S (0.5 ml) and CH2Cl2 (6 ml) was stirred at room temperature over night. The yield after purification was quantitative.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07288571B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-c760587af0a9433796156797d7a55326 |
| Source note | uspto-grants-2007_10 |