HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 58982139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 2-Bromomethylnaphthalene | HCID 70320 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58982139 | HCID 58982139 | 97% |
Reaction Steps
Following the procedure described in Example 122, step 1, but substituting respectively 2-bromomethylnaphthalene for methyl iodide, and DMF for THF, the title compound 217 was obtained in 97% yield. MS (ESI)=254 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07288567B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-c7ac6b1be47e45fe9c6aedf018ae421e |
| Source note | uspto-grants-2007_10 |