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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1182583Generated: November 2, 2026

Acetone → HCID 10117784, compound

https://huagongshe.com/reaction/1182583

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetoneHCID 180—
ReactantHCID 9827369HCID 9827369—
ReactantAmmonium cerium-nitrateHCID 57418452—
SolventWaterHCID 962—
ProductHCID 10117784HCID 10117784—

Reaction Steps

2 ml of acetone was added to 50.7 mg (0.100 mmol) of 4-(3-chlorophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid mono (3,3-diphenylpropyl) ester. 130 mg (0.240 mmol) of cerium ammonium nitrate suspended in 1 ml of water was added and stirred at room temperature for 10 minutes. After adding water and extracting with ethyl acetate, the organic layer was dried over anhydrous sodium sulfate and then concentrated under reduced pressure to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07288544B2
Source datasetuspto-grants-2007_10
ORD IDord-d61cd7e67bd941c0802c1c93b953cac9
Source noteuspto-grants-2007_10