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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1182590Generated: November 3, 2026

Hydrochloric Acid → HCID 86590785, compound

https://huagongshe.com/reaction/1182590

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantWaterHCID 962—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 86590784HCID 86590784—
SolventMethanolHCID 887—
ProductHCID 86590785HCID 86590785—

Reaction Steps

250 mg (0.390 mmol) of 6-(2-azidoethoxy) methyl-4-(3-chlorophenyl)-5-(3,3-diphenylpropylcarbamoyl)-2-methyl-1,4-dihydropyridine-3-carboxylic acid (2-cyanoethyl) ester was dissolved in 2 ml of methanol. 0.70 ml of 1 N aqueous sodium hydroxide solution was added and stirred at room temperature for 8 hours. After adding 1 N hydrochloric acid and water, precipitates thus formed were taken by the filtration and dried under reduced pressure to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07288544B2
Source datasetuspto-grants-2007_10
ORD IDord-727855d407194dd1a0a0f2d031238067
Source noteuspto-grants-2007_10