Chlorosuccinimide → HCID 57514541, compound

HRID 1182902Notes

Reaction equation

HRID 1182902 reaction equation
[CH3:1][N:2]1[C:11](=[O:12])[C:10]2[N:9]([CH2:13][C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=3[C:20]#[N:21])[CH:8]=[N:7][C:6]=2[N:5]([CH2:22][O:23][CH2:24][CH2:25][Si:26]([CH3:29])([CH3:28])[CH3:27])[C:3]1=[O:4].[Cl:30]N1C(=O)CCC1=O>ClC(Cl)C>[CH3:1][N:2]1[C:11](=[O:12])[C:10]2[N:9]([CH2:13][C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=3[C:20]#[N:21])[C:8]([Cl:30])=[N:7][C:6]=2[N:5]([CH2:22][O:23][CH2:24][CH2:25][Si:26]([CH3:28])([CH3:27])[CH3:29])[C:3]1=[O:4]

Participants

4

Reactant 2

HCID 31398ChlorosuccinimideHCID 53629009HCID 53629009, compound

Product 1

HCID 57514541HCID 57514541, compound

Reagents, catalysts & solvents 1

HCID 63651,1-DichloroethaneSolvent

Procedure

Prepared by chlorination of 1-methyl-3-[(2-trimethylsilanyl-ethoxy)methyl]-7-(2-cyano-benzyl)-xanthine with N-chlorosuccinimide in dichloroethane while refluxing.

Workup

  1. temperaturewhile refluxing

Sources & evidence

ORD record
ord-cd77f9fb97b54e53b4d833b5efd1aeac
Source dataset
uspto-grants-2014_03
Patent number
US08664232B2

Reaction notes

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