HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → HCID 53327292, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | HCID 67294292 | HCID 67294292 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53327292 | HCID 53327292 | — |
Reaction Steps
5.0 mL of hydroxylamine solution (50 wt. % in water) was added to a solution of 0.169 g of methyl 5-(4-fluorobenzyl)-3-hydroxy-4-methylpicolinate 7c (0.615 mmol, 1 eq) in 5.0 mL of tetrahydrofuran. The reaction mixture was stirred at reflux overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08664248B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-852508cd7a8a4e1d99f9eafc8ade5636 |
| Source note | uspto-grants-2014_03 |