HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 67362326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 67362940 | HCID 67362940 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67362326 | HCID 67362326 | 58% |
Reaction Steps
The crude compound obtained in step 1 was dissolved in 10 ml of methanol. 1.4 ml of an aqueous 1 M solution of sodium hydroxide were added and the mixture was stirred overnight at room temperature. The solvent was removed in vacuo and the residue purified by preparative HPLC to give 102 mg (58%) of the title compound
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08664257B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-b9687e65b3084772ba68d088d01d04eb |
| Source note | uspto-grants-2014_03 |