HRID1183196

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID53395981

未命名化合物

HCID67204676

未命名化合物

PRODUCTS

生成物

结构：C(=Cc1ccc(N(c2ccccc2)c2ccc3oc4ccccc4c3c2)cc1)c1ccc(N(c2ccccc2)c2ccc3oc4ccccc4c3c2)cc1

HCID68109724

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID21226206

未命名化合物

PROCEDURE

实验过程

The Rf values of the object of the synthesis, 4,4′-dibromostilbene, and (dibenzofuran-2-yl)-phenylamine were respectively 0.37, 0.62, and 0.31, which were found by silica gel thin layer chromatography (TLC) (ethyl acetate:hexane (1:10) as the developing solvent).

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-fb94fe00aaea462a81b4c37cff3a3e99
来源数据集: uspto-grants-2014_03
DOI: 10.6084/m9.figshare.5104873.v1
专利: US08664263B2
来源说明: uspto-grants-2014_03

反应 SMILES

Br[C:2]1[CH:7]=[CH:6][C:5]([CH:8]=[CH:9][C:10]2[CH:15]=[CH:14][C:13](Br)=[CH:12][CH:11]=2)=[CH:4][CH:3]=1.[CH:17]1[C:25]2[C:24]3[CH:26]=[CH:27][CH:28]=[CH:29][C:23]=3[O:22][C:21]=2[CH:20]=[CH:19][C:18]=1[NH:30][C:31]1[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1>C(OCC)(=O)C.CCCCCC>[CH:17]1[C:25]2[C:24]3[CH:26]=[CH:27][CH:28]=[CH:29][C:23]=3[O:22][C:21]=2[CH:20]=[CH:19][C:18]=1[N:30]([C:2]1[CH:7]=[CH:6][C:5]([CH:8]=[CH:9][C:10]2[CH:15]=[CH:14][C:13]([N:30]([C:31]3[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=3)[C:18]3[CH:19]=[CH:20][C:21]4[O:22][C:23]5[CH:29]=[CH:28][CH:27]=[CH:26][C:24]=5[C:25]=4[CH:17]=3)=[CH:12][CH:11]=2)=[CH:4][CH:3]=1)[C:31]1[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1