HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4'-Dibromostilbene → 4,4'-bis[N-(dibenzofuran-2-yl)-N-phenylamino]stilbene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4'-Dibromostilbene | HCID 53395981 | — |
| Reactant | N-phenyl-2-Dibenzofuranamine | HCID 67204676 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | 4,4'-bis[N-(dibenzofuran-2-yl)-N-phenylamino]stilbene | HCID 68109724 | — |
Reaction Steps
The Rf values of the object of the synthesis, 4,4′-dibromostilbene, and (dibenzofuran-2-yl)-phenylamine were respectively 0.37, 0.62, and 0.31, which were found by silica gel thin layer chromatography (TLC) (ethyl acetate:hexane (1:10) as the developing solvent).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08664263B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-fb94fe00aaea462a81b4c37cff3a3e99 |
| Source note | uspto-grants-2014_03 |