HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Benzeneacetic acid, hydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Methyl phenylacetate | HCID 7559 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Product | Benzeneacetic acid, hydrazide | HCID 70301 | — |
Reaction Steps
Phenyl-acetic acid methyl ester (5 g, 33.3 mmol) was dissolved in hydrazine hydrate (25 mL) and EtOH (50 mL) and the reaction was heated in a sealed tube to 80° C. overnight. After cooling the reaction was concentrated to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08664220B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-e77343450d5f47a48e97d4b5d67004de |
| Source note | uspto-grants-2014_03 |