HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 2-Benzenesulfinyl-6-bromo-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 2-Bromo-6-phenylsulfanylpyridine | HCID 824591 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Benzenesulfinyl-6-bromo-pyridine | HCID 86679095 | — |
Reaction Steps
2-Bromo-6-phenylsulfanyl-pyridine (0.5323 g, 2 mmol) was dissolved in CH2Cl2 (20 mL) and m-chloroperbenzoic acid (0.345 g, 2 mmol) was added. The reaction was stirred at room temperature overnight then submitted to aqueous workup and purification on silica gel to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08664220B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-26914c45d55841a4a736b549738cd277 |
| Source note | uspto-grants-2014_03 |