HCID 24814178, compound → HCID 24814179, compound

Participants

Reaction Steps

MnO2 (40 mg, 444 μmol) is added to a solution of compound 8 (27 mg, 74 μmol) in dichloromethane (2 ml). The suspension obtained is stirred for 48 hours at room temperature and then it is filtered. The solid obtained is washed with dichloromethane. The mother liquors are then concentrated to give 25 mg of compound 9 in the form of a yellow solid (yield: 91%).

Provenance & Evidence