Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1183836Generated: November 2, 2026

Acrylic Acid → 3-(Ethylbutoxyphosphinyl)propionic acid

https://huagongshe.com/reaction/1183836

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcrylic AcidHCID 6581—
ReactantButyl ethyiphosphoniteHCID 86614949—
SolventTolueneHCID 1140—
Product3-(Ethylbutoxyphosphinyl)propionic acidHCID 8665668091%

Reaction Steps

149 g (1 mol) of butyl ethylphosphonite (produced as in Example 2) and 86 g (1.2 mol) of acrylic acid in 217 g of toluene are heated to about 100° C. While stirring, 124 g of a 10% strength solution of WakoV65 in toluene are metered in. The solvent is distilled off in vacuo to leave 201 g (91% of theory) of 3-(ethylbutoxyphosphinyl)propionic acid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08664418B2
Source datasetuspto-grants-2014_03
ORD IDord-4b0174bea32145b9965c8ad7552159b8
Source noteuspto-grants-2014_03