Chlorodimethylsilane → HCID 178504351, compound

HRID 1183846Notes

Reaction equation

HRID 1183846 reaction equation
Cl[CH2:2][CH2:3][CH2:4][CH2:5][C-:6]1[CH:10]=[CH:9][CH:8]=[CH:7]1.[CH-:11]1[CH:15]=[CH:14][CH:13]=[CH:12]1.[Fe+2:16].[Mg].Cl[SiH:19]([CH3:21])[CH3:20]>>[CH3:20][SiH:19]([CH3:21])[CH2:2][CH2:3][CH2:4][CH2:5][C-:6]1[CH:10]=[CH:9][CH:8]=[CH:7]1.[CH-:11]1[CH:15]=[CH:14][CH:13]=[CH:12]1.[Fe+2:16]

Participants

4

Reactant 3

HCID 66108ChlorodimethylsilaneHCID 5462224MagnesiumHCID 15346559Chlorobutyl ferrocene

Product 1

HCID 178504351HCID 178504351, compound

Procedure

In the third reaction stage 4-chlorobutylferrocene was reacted with magnesium metal under Grignard type reaction conditions to form the corresponding Grignard intermediate compound which reacted with chlorodimethylsilane in-situ to give 4-(dimethylsilyl)butylferrocene

Workup

  1. customto form the corresponding Grignard intermediate compound which

Sources & evidence

ORD record
ord-9316fa227a0044ef853087b5ec205af4
Source dataset
uspto-grants-2014_03
Patent number
US08664417B2

Reaction notes

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