HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-dihydro-4-methyl-2H-1,4-benzoxazine-2-carboxamide → Dihydro-8-carbamoyl-2H-1,4-benzoxazine-2-methanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-dihydro-4-methyl-2H-1,4-benzoxazine-2-carboxamide | HCID 12826552 | — |
| Reactant | Dihydro-8-fluoro-2H-1,4-benzoxazine-2-methanamine | HCID 67497870 | — |
| Product | Dihydro-8-carbamoyl-2H-1,4-benzoxazine-2-methanamine | HCID 67497746 | — |
Reaction Steps
This compound is obtained following the same experimental conditions as those used for the synthesis of intermediate (2b) but replacing 3,4-dihydro-8-fluoro-2H-1,4-benzoxazine-2-carboxamide (4b) with 3,4-dihydro-4-methyl-2H-1,4-benzoxazine-2-carboxamide (4h). The title compound of formula (2h) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669250B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-8b19fd049afa4c78b431703f966fe0be |
| Source note | uspto-grants-2014_03 |