HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 86680541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 2-Fluoroethylamine | HCID 9996 | — |
| Reactant | HCID 86680539 | HCID 86680539 | — |
| Product | HCID 86680541 | HCID 86680541 | — |
Reaction Steps
The title compound was prepared as a trifluoroacetic acid salt according to the procedure described in Example 194B, substituting the product from Example 179A for the product from Example 194A, and substituting 2-fluoroethanamine for ethylamine 1H NMR (300 MHz, CDCl3) δ ppm 0.88-1.06 (m, 4 H) 4.62-4.77 (m, 1 H) 4.78-4.93 (m, 1 H) 5.42-5.71 (m, 1 H) 7.63-7.76 (m, 3 H) 7.77-7.86 (m, 1 H) 7.88-7.95 (m, 1 H) 7.98-8.14 (m, 1 H); MS (ESI) m/z 508 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669255B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-36479d1e20444db3ad7c308bfb700af0 |
| Source note | uspto-grants-2014_03 |