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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1184622Generated: November 1, 2026

Ethylamine → HCID 86680541, compound

https://huagongshe.com/reaction/1184622

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthylamineHCID 6341—
ReactantTrifluoroacetic acidHCID 6422—
Reactant2-FluoroethylamineHCID 9996—
ReactantHCID 86680539HCID 86680539—
ProductHCID 86680541HCID 86680541—

Reaction Steps

The title compound was prepared as a trifluoroacetic acid salt according to the procedure described in Example 194B, substituting the product from Example 179A for the product from Example 194A, and substituting 2-fluoroethanamine for ethylamine 1H NMR (300 MHz, CDCl3) δ ppm 0.88-1.06 (m, 4 H) 4.62-4.77 (m, 1 H) 4.78-4.93 (m, 1 H) 5.42-5.71 (m, 1 H) 7.63-7.76 (m, 3 H) 7.77-7.86 (m, 1 H) 7.88-7.95 (m, 1 H) 7.98-8.14 (m, 1 H); MS (ESI) m/z 508 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08669255B2
Source datasetuspto-grants-2014_03
ORD IDord-36479d1e20444db3ad7c308bfb700af0
Source noteuspto-grants-2014_03