HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl chloroformate → 4-(5-Chloro-2,3-dihydro-furo[2,3-c]pyridin-2-yl)-piperidine-1-carboxylic acid isopropyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl chloroformate | HCID 7917 | — |
| Reactant | 5-Chloro-2-piperidin-4-yl-2,3-dihydro-furo[2,3-c]pyridine | HCID 86674898 | — |
| Product | 4-(5-Chloro-2,3-dihydro-furo[2,3-c]pyridin-2-yl)-piperidine-1-carboxylic acid isopropyl ester | HCID 86674897 | — |
Reaction Steps
The title compound is prepared from 5-chloro-2-piperidin-4-yl-2,3-dihydro-furo[2,3-c]pyridine and isopropyl chloroformate following a procedure analogous to that described in Example 4. LC (method 7): tR=1.37 min; Mass spectrum (ESI+): m/z=325 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669271B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-f60c09ddffa549f58da5a28e1b475191 |
| Source note | uspto-grants-2014_03 |