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HRID1184789

反应详情

EQUATION

反应方程式

HRID 1184789 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CC(C)S(=O)(=O)Cl
HCID82408

Isopropyl sulfonyl chloride

C3H7ClO2S

结构：CC(C)(C)OC(=O)N1CCC(C2Cc3cc(N4CCNCC4)ncc3O2)CC1
HCID67973467

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)S(=O)(=O)N1CCN(c2cc3c(cn2)OC(C2CCN(C(=O)OC(C)(C)C)CC2)C3)CC1
HCID67990227

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

The title compound is prepared by treatment of 4-(5-piperazin-1-yl-2,3-dihydro-furo[2,3-c]pyridin-2-yl)-piperidine-1-carboxylic acid tert-butyl ester with isopropylsulfonyl chloride in dichloromethane in the presence of triethylamine. LC (method 10): tR=1.48 min; Mass spectrum (ESI+): m/z=495 [M+H]+.