HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 19990247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 5-chloro-1-methyl-4-nitro-1H-pyrazole | HCID 12344836 | — |
| Product | HCID 19990247 | HCID 19990247 | 100% |
Reaction Steps
Reaction of 5-chloro-1-methyl-4-nitro-1H-pyrazole and dimethylamine gave N,N,1-trimethyl-4-nitro-1H-pyrazol-5-amine as a yellow solid (210 g, 100%). 1H NMR (400 MHz, CDCl3) δ 8.01 (s, 1H), 3.75 (s, 3H), 2.90 (s, 6H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669361B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-c3f20e1dfd284f2aaf93700e1c4882d1 |
| Source note | uspto-grants-2014_03 |