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HRID1185573

反应详情

EQUATION

反应方程式

HRID 1185573 的结构方程式

REACTANTS

反应物

1
结构：CCCCOC(=O)N1CCN(C(=O)[C@H](Cc2cn(Cc3ccccc3)nn2)NC(=O)OC(C)(C)C)CC1
HCID68598891

未命名化合物

PRODUCTS

生成物

1
结构：CCCCOC(=O)N1CCN(C(=O)[C@H](Cc2c[nH]nn2)NC(=O)OC(C)(C)C)CC1
HCID178452367

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CO
溶剂HCID887

Methanol

CH4O

结构：[OH-].[OH-].[Pd+2]
溶剂HCID9942167

Palladium hydroxide

H2O2Pd

PROCEDURE

实验过程

Debenzylation of 4-[(S)-3-(1-Benzyl-1H-[1,2,3]triazol-4-yl)-2-tert-butoxycarbonylamino-propionyl]-piperazine-1-carboxylic acid butyl ester (1.14 g) was performed using the H-Cube® (Thales Nanotechnology). Parameters were chosen as follows: 0.05 M solution in MeOH, Pd(OH)2/C, 60° C., 30 bar. Yield: 739 mg colorless foam.