HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68599078, compound → 4-Carboxymethoxy-7-methyl-quinoline-2-carboxylic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68599078 | HCID 68599078 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Carboxymethoxy-7-methyl-quinoline-2-carboxylic acid methyl ester | HCID 68598932 | — |
Reaction Steps
To a solution of 3.00 g 4-Benzyloxycarbonylmethoxy-7-methyl-quinoline-2-carboxylic acid methyl ester in 50 ml ethanol were added under argon 0.3 g Pd/C (10%) and the suspension was stirred under an atmosphere of hydrogen (3 bar) for 16 h. The suspension was filtered over a plug of Celite® and washed with ethanol. The crude product was obtained after evaporation of the solvent. Yield: 1.90 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669266B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-48306bd95ebb44f087f8edfcdfb127cf |
| Source note | uspto-grants-2014_03 |