HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylsilyldiazomethane → Methyl 2-(2,4-dinitrophenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylsilyldiazomethane | HCID 167693 | — |
| Reactant | 2,4-Dinitrophenylacetic acid | HCID 221513 | — |
| Product | Methyl 2-(2,4-dinitrophenyl)acetate | HCID 286146 | — |
Reaction Steps
2,4-diaminophenylacetic acid methyl ester is obtained by reacting 2,4-dinitrophenylacetic acid with trimethylsilyldiazomethane to obtain 2,4-dinitrophenylacetic acid methyl ester, followed by reducing 2,4-dinitrophenylacetic acid methyl ester using a strong reducing agent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673177B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-81851434d0124e648183b204fc35fc39 |
| Source note | uspto-grants-2014_03 |