HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia methanol → HCID 131731245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia methanol | HCID 21705897 | — |
| Reactant | HCID 71245451 | HCID 71245451 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131731245 | HCID 131731245 | 84% |
Reaction Steps
To a solution of compound 6 (250 g, 0.42 mmol) in CH3OH (2 mL) was added MeOH—NH3 (10 mL) and was stirred at RT for 16 h. The volatiles were evaporated under reduced pressure to afford compound 7 (190 mg, 84%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673843B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-36ee3a6efa6d432fa99ae504ff9df0f4 |
| Source note | uspto-grants-2014_03 |