Methyl iodide → HCID 67401538, compound

Participants

Reaction Steps

3-(1,3-Dioxolan-2-yl)pyridine (1.00 g, 6.62 mmol) was dissolved in dichloromethane (20.0 mL). To this, iodomethane (494 μL, 7.94 mmol) was added under a nitrogen atmosphere at room temperature and the mixture was stirred at room temperature for 72 hours. The reaction mixture was concentrated, and the residue was subjected to slurry purification using diisopropyl ether, to give 3-(1,3-dioxolan-2-yl)-1-pyridinium iodide (1.85 g, yield: 96%).

Provenance & Evidence