Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Sulfite | HCID 24437 | — |
| Reactant | Bromomethylcyclopropane | HCID 81503 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86622428 | HCID 86622428 | 128.9% |
Reaction Steps
Sodium sulfite (1.43 g, 11.3 mmol) was dissolved in water (8.00 mL). To this, (bromomethyl)cyclopropane (1.00 mL, 10.3 mmol) was added and the mixture was stirred with heat at 100° C. for 24 hours. The solvent in the reaction mixture was evaporated off under reduced pressure, and the residue was subjected to slurry purification using diisopropyl ether, to give sodium cyclopropanemethanesulfonate (2.10 g, yield: 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08673908B2 |
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| Source dataset | uspto-grants-2014_03 |
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| ORD ID | ord-6d93072c963547d6a12f618a3967d262 |
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| Source note | uspto-grants-2014_03 |
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