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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1186448Generated: November 2, 2026

Sodium Sulfite → HCID 86622428, compound

https://huagongshe.com/reaction/1186448

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium SulfiteHCID 24437—
ReactantBromomethylcyclopropaneHCID 81503—
SolventWaterHCID 962—
ProductHCID 86622428HCID 86622428128.9%

Reaction Conditions

Temperature100 °C

Reaction Steps

Sodium sulfite (1.43 g, 11.3 mmol) was dissolved in water (8.00 mL). To this, (bromomethyl)cyclopropane (1.00 mL, 10.3 mmol) was added and the mixture was stirred with heat at 100° C. for 24 hours. The solvent in the reaction mixture was evaporated off under reduced pressure, and the residue was subjected to slurry purification using diisopropyl ether, to give sodium cyclopropanemethanesulfonate (2.10 g, yield: 99%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08673908B2
Source datasetuspto-grants-2014_03
ORD IDord-6d93072c963547d6a12f618a3967d262
Source noteuspto-grants-2014_03