HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-amino-N-(2-methylphenyl)benzene-1-sulfonamide → HCID 43257989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-amino-N-(2-methylphenyl)benzene-1-sulfonamide | HCID 593569 | — |
| Reactant | HCID 58398228 | HCID 58398228 | — |
| Product | HCID 43257989 | HCID 43257989 | 93% |
Reaction Steps
(RK2-065-01) I This compound was prepared according to the procedure described for compound 12a except using 11j to obtain the required product as a yellow solid (63 mg, 93%). Mp=189-191° C.; 1H NMR (400 MHz, CD3OD) δ 7.30 (d, J=8.8 Hz, 1H), 7.10-7.06 (m, 2H), 7.01-6.97 (m, 2H), 6.31 (d, J=1.6 Hz, 1H), 6.12 (dd, J=8.8, 2.0 Hz, 1H), 3.30 (s, 3H), 2.22 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673910B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-0eee0e44ebdc4c94977049b5662d4202 |
| Source note | uspto-grants-2014_03 |