huagongshe.com
HRID1186657

反应详情

EQUATION

反应方程式

HRID 1186657 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(N)(=O)=O)cc1
HCID6269

4-Toluenesulfonamide

C7H9NO2S

结构：CCOC(=O)CSC1=C/C(=N\S(=O)(=O)c2cccs2)c2ccccc2C1=O
HCID58398202

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)CSC1=CC(=NS(=O)(=O)c2ccc(C)cc2)c2ccccc2C1=O
HCID67330702

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Cl][Ti]([Cl])([Cl])[Cl]
催化剂HCID24193

Titanium tetrachloride

Cl4Ti

结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

5.2.20 Ethyl 2-(1-oxo-4-(tosylimino)-1,4-dihydronaphthalen-2-ylthio)acetate (81) was prepared according to the procedure for 8a except using 4-methylbenzenesulfonamide, TiCl4.2THF and THF as solvent. The title compound 100.7 mg (46.9%) was obtained according to the workup procedure for 12a as a yellow solid, m.p.: ° C.