HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Mercaptobenzoic Acid → 2-(1-Hydroxy-4-(thiophene-2-sulfonamido)naphthalen-2-ylthio)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Mercaptobenzoic Acid | HCID 5443 | — |
| Reactant | 2-{[1-Hydroxy-4-(thiophene-2-sulfonamido)naphthalen-2-yl]sulfanyl}acetic acid | HCID 1582605 | — |
| Product | 2-(1-Hydroxy-4-(thiophene-2-sulfonamido)naphthalen-2-ylthio)benzoic acid | HCID 44609145 | — |
Reaction Steps
5.2.54 2-(1-hydroxy-4-(thiophene-2-sulfonamido)naphthalen-2-ylthio)benzoic acid (14l) was prepared according to the procedure of procedure B for 10a except using thiosalicylic acid, which afforded the title compound 19 mg (99%) as a white solid, m.p.: 215° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673910B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-73902e3694fe4680a9ae54b94b11702d |
| Source note | uspto-grants-2014_03 |