HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58121056, compound → tert-Butyl (2-amino-4-(thiophen-2-yl)phenyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58121056 | HCID 58121056 | — |
| Reactant | tert-Butyl 2-nitro-4-(thiophen-2-yl)phenylcarbamate | HCID 59736984 | — |
| Product | tert-Butyl (2-amino-4-(thiophen-2-yl)phenyl)carbamate | HCID 57717474 | 92% |
Reaction Steps
The procedure was followed as outlined in Scheme 3, Step 3 replacing compound 37 with compound 60 to afford tert-butyl 2-amino-4-(thiophen-2-yl)phenylcarbamate 61 (2.75 g, 92% yield) as a yellow solid. LRMS (ESI): (calc.) 290.11 (found) 235.1 (M(-tBu)Na)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673911B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-5a9b0b950b6b4e85b83360c53dd80503 |
| Source note | uspto-grants-2014_03 |